76735
O-(2,3,4,5,6-Pentafluorobenzyl)hydroxylamine hydrochloride
derivatization grade (GC derivatization), LiChropur™, ≥99.0% (AT)
Synonym(s):
PFBHA·HCl
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About This Item
Linear Formula:
C6F5CH2ONH2·HCl
CAS Number:
Molecular Weight:
249.57
UNSPSC Code:
23151817
NACRES:
NA.22
PubChem Substance ID:
EC Number:
261-057-7
Beilstein/REAXYS Number:
4031190
MDL number:
Assay:
≥99.0% (AT)
Form:
solid
grade
derivatization grade (GC derivatization)
Quality Level
assay
≥99.0% (AT)
form
solid
quality
LiChropur™
reaction suitability
reagent type: derivatization reagent
reaction type: Alkylations
technique(s)
gas chromatography (GC): suitable
mp
212-218 °C, 227 °C (subl.) (lit.)
solubility
H2O: 5%, clear
SMILES string
Cl.NOCc1c(F)c(F)c(F)c(F)c1F
InChI
1S/C7H4F5NO.ClH/c8-3-2(1-14-13)4(9)6(11)7(12)5(3)10;/h1,13H2;1H
InChI key
HVMVKNXIMUCYJA-UHFFFAOYSA-N
General description
O-(2,3,4,5,6-Pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA.HCl) is a derivatizing agent.
Application
PFBHA.HCl has been used for derivatization of metabolites with carbonyl groups followed by analysis via GC-MS. It has also been used in aldehyde derivatization followed by aldehydic hydrolysis using GC/MS.
Packaging
Bottomless glass bottle. Contents are inside inserted fused cone.
Other Notes
Sensitive derivatizing agent for electron capture gas chromatographic analysis of carbonyl-containing compounds: keto steroids and carbohydrates
Legal Information
LiChropur is a trademark of Merck KGaA, Darmstadt, Germany
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Storage Class
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
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Plasmalogen degradation by oxidative stress: production and disappearance of specific fatty aldehydes and fatty alpha-hydroxyaldehydes.
Stadelmann-Ingrand S
Free Radical Biology & Medicine, 31(10), 1263-1271 (2001)
Yun-Gon Kim et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 893-894, 177-181 (2012-03-31)
Nucleotide diphosphate (NDP) sugars are widely present in antibiotics and glycoconjugates, such as protein- and lipid-linked oligosaccharides, where they act as substrates for glycosyltransferase in eukaryotes and prokaryotes. Among NDP sugars, NDP-4-keto sugars are key intermediates in the synthesis of
Chunhui Deng et al.
Rapid communications in mass spectrometry : RCM, 19(5), 647-653 (2005-02-09)
In the current work, a simple, rapid, accurate and inexpensive method was developed for the determination of acetone in human blood. The proposed method is based on derivatization with O-(2,3,4,5,6-pentafluorobenzyl)hydroxylamine hydrochloride (PFBHA), followed by headspace liquid-phase microextraction (HS-LPME) and gas
Global Trade Item Number
| SKU | GTIN |
|---|---|
| 76735-10X1G | 04061832924120 |
| 76735-1G-KC | 04061826492062 |
| 76735-1G | 04061832924175 |