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Merck
CN

55506-U

Supel QuE QuEChERS tube

Z-Sep/C18 Tube, pk of 50, centrifuge tube volume 15 mL , Shaker Compatible

Synonym(s):

QuEChERS

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21
Material:
polypropylene tube
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Product Name

Supel QuE, Z-Sep/C18 Tube, pk of 50, centrifuge tube volume 15 mL , Shaker Compatible

material

polypropylene tube

Quality Level

product line

Supel

composition

Discovery® DSC-18, 300 mg , Z-Sep, 120 mg

packaging

pk of 50

technique(s)

QuEChERS: suitable

centrifuge tube volume

15 mL , Shaker Compatible

matrix active group

zirconia-based phase

application(s)

food and beverages

compatibility

for use with most QuEChERS shakers

General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Other Notes

Supel QuE Z-Sep products enhance sample cleanup for complex matrices by effectively removing more fat and color from sample extracts than traditional phases for QuEChERS methods. By eliminating problematic matrix interferences, Z-Sep products provide more robust LC-MS and GC-MS methods. This proprietary technology can replace C18 and PSA in your current methods without additional method development.

Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.

Legal Information

Certain uses of this product may be covered by the claims of one or more pending patent applications. For licensing inquiries please contact techserv@sial.com
AOAC is a registered trademark of AOAC International
Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supel is a trademark of Sigma-Aldrich Co. LLC


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Storage Class

11 - Combustible Solids

wgk

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable



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Related Content


Lianzhu Wang et al.
Se pu = Chinese journal of chromatography, 33(5), 501-507 (2015-09-22)
A fast method based on QuEChERS methodology for the simultaneous determination of 32 sulfonylurea herbicide residues in sweet corns and green soybeans was developed using liquid chromatography-tandem mass spectrometry (LC-MS/MS). The clean-up effects of three dispersive sorbents were evaluated in
Darina Lankova et al.
Analytical and bioanalytical chemistry, 408(10), 2515-2525 (2016-02-11)
In this study, a novel analytical approach for the determination of 11 monohydroxylated polycyclic aromatic hydrocarbon metabolites (OH-PAHs) in urine was developed and validated. The rapid, simple and high-throughput sample preparation procedure based on ethyl acetate extraction and subsequent purification
Hui Li et al.
Journal of chromatography. A, 1528, 53-60 (2017-11-07)
Herein, an accurate and reliable isotope-labelled internal standard method was developed and validated for simultaneous determination of three polar pesticide adjuvants, namely 2-pyrrolidone, N-methyl-2-pyrrolidone, and N-ethyl-2-pyrrolidone in plant-derived agro-products. Matrices, including apple, cabbage, tomato, cucumber, rice, and wheat were extracted



Global Trade Item Number

SKUGTIN
55506-U04061833528792